Delamination and buckling induced by compressive strain in. Delamination of thin film strips home page harvard. Accordingly, an uniaxial compression test was designed to trigger film buckling and interface cracking in titindu systems. Instabilities of thin films on a compliant substrate. This is demonstrated experimentally by observing both the buckling modes and a mode transition in a single filmsubstrate system with varying stress and interfacial defects. Interactive study of straightsided buckling patterns in. In this thesis, we focus on the buckling mechanism. Thinwalled, coldformed steel members exhibit a complicated postbuckling regime that is difficult to predict. The pattern formation during delamination and buckling in sputterdeposited tungsten thin films under large compressive stresses was investigated. N2 we consider the deformation of a thin elastic film bonded to a thick compliant substrate, when the compressive misfit is far beyond critical. Currently, the most commonly used techniques to assess interface properties of a thin film on a compliant substrate is to use bending experiments or uniaxial tensile straining to induce film fracture and delamination in the form of buckles. The mechanisms whereby these debonding patterns interact have been investigated taking into account the elastic energy. T1 analysis of a compressed thin film bonded to a compliant substrate.
Experimental and numerical investigation of buckling and. Department of electrical and computer engineering, university of california, davis, ca, usa. In order to simulate the thin films which subjected to compound loads and the buckle modes. Buckling, wrinkling and debonding in thin film systems.
However, no systematic study devoted to the determination of the interface adhesion of thin films exists and main factors influencing it was carried out so far. Based on this approach, formation of complex 3d configurations with suspended curvy features or hierarchical geometries remains a challenge. Four block samples were used in this test and the test procedure is illustrated in fig. Adhesiongoverned buckling of thinfilm electronics on soft tissues. Detailed modelling of delamination buckling of thin films under. We begin with the compressive buckling of thin films. Postbuckling of a thin film strip delamination in a. Behavior of thinfilmtype delamination of layered composite.
The buckling analysis in sections 2 the finite deformation buckling analysis for stiff thin films on compliant substrates, 3 perturbation analysis of the substrate is for the stiff thin film compliant substrate system subjected to the prestrain. The first is characterized by a domed shape that continues into an x, or saltire, under higher stress. We consider the deformation of a thin elastic film bonded to a thick compliant substrate, when the compressive misfit is far beyond critical. Postbuckling solutions are obtained for a laminate with clamped ends applicable to thin film strip delamination in a base laminate under uniform membrane loads. Curved, thin, flexible complex threedimensional 3d structures can be very hard to manufacture at small length scales. Us10538028b2 deterministic assembly of complex, three.
Delamination of compressively loaded composite laminates in the context of design. Oct 02, 2007 depositing a film onto a heated substrate and then cooling the system lead to compressive strains in the film when its coefficient of thermal expansion is smaller than that of the substrate. As a stressdriven instability, the study of buckling can be traced back to the classical euler buckling of an elastic column. Buckling delamination appears to be a multiscale phenomenon. Buckling of a stiff thin film on an elastic graded compliant. The wrinkling of a stiff thin film bonded on a soft elastic layer and subjected to an applied or residual compressive stress is investigated in the. Quantifying strain via buckling instabilities in surface. Straightsided buckling patterns arise perpendicular to the compression axis which tend to attract one another during propagation a few hundred nanometers apart. Buckling of a stiff thin film on an elastic graded. Electrical and optical properties of the transferable ga 2 o 3 thin films exhibit a potential for application in solar.
A revision of the basic assumptions those are usually used in the analysis of stability of thin delaminated layer and delamination propagation in a compressed composite is presented in this paper. Herringbone buckling patterns of compressed thin films on compliant substrates a thin metal. Finite deformation mechanics in buckled thin films on. Formation of buckles wrinkles on a thin film attached to a compliant substrate has received considerable attention due to the advancement of flexible electronics, 1 5 optoelectronics and photovoltaics, 6 11 and various functional devices, 12 16 as well as the development of selforganizing mechanisms. Active, expires 20371108 application number us14944,039 other versions. Sufficiently large compression leads to buckling instabilities in the film that create wavy deformations i. Over the last several decades, numerous theoretical and experimental studies of this phenomenon have been performed 117. For films or coatings deposited on substrate at high temperature, residual compressive stresses are often induced in the surface layers because of the mismatch in the thermal expansion coefficients. N2 we consider the deformation of a thin elastic film bonded to a thick compliant substrate, when the. Buckling based on specific patterns can be divided into 2, 3.
Spontaneous delamination via compressive buckling facilitates. In order to simulate the thin films which subjected to compound loads and the buckle modes the external uniaxial compression and thermal. The steadystate ener gy release rate for full delamination of the strip equals the average. The mechanically guided assembly that relies on the compressive buckling of strategically patterned 2d thin films represents a robust route to complex 3d mesostructures in advanced materials and. Although buckling has historically been viewed as a mechanism for structural failure, pioneering work in the late 1990s showed that this behavior can be. Releasing the prestrain leads to compressive strains on the ribbons that generate the wavy layouts. Thinfilm buckling buckle generally considered refers to a failure mode caused by the compressive force on the film material, characterized by the vertical displacement perpendicular to load direction. The prestrain is usually generated by one of two methods. Fracture, delamination, and buckling of elastic thin films on. Using a scanning xray microdiffraction technique developed at a third generation xray synchrotron source, we obtained. Pdf buckling of thin films in nanoscale researchgate. Residual andor externally applied stresses in thin films can cause film fracture. Here, the effect of moisture, which presence decreases film adhesion, was quantified for dlc and copper films.
Even when stresses do not cause catastrophic failure, they seriously impact device performance. Reprogrammable 3d mesostructures through compressive. Tensile specimens of metal films on compliant substrates are widely used for. For this purpose, the theory of flexible elastic plates with large displacements was used. Telephone cord delaminations have been observed in several film systems 812, including commercial. Interactive study of straightsided buckling patterns in thin. For most applications a film with low tensile stress or no stress at all is desired. Buckling and cracking of thin films on compliant substrates under compression. Fracture, delamination, and buckling of elastic thin films. In the case of compressive stress thin film buckling is observed in the form of delamination blisters, which can be either circular, straight, or form periodic buckling patterns commonly. Until recently, the small dimensions of the buckling have prevented measurements of their local in plane internal stress distribution. Buckling and postbuckling of delaminated composites under. Thin film, buckling, elastic mismatch, compliant substrate. Today, advanced computational modeling supplements experimental investigation.
An analytic model of twolevel compressive buckling with. The ga 2 o 3 films optical band gap and schottky barrier height with gold are 4. As the system is further cooled, a highly ordered herringbone pattern has been observed to develop. An analytical model is established for the buckling of a stiff thin film on a semiinfinite elastic graded compliant substrate subjected to inplane compression.
Herringbone buckling patterns of compressed thin films. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed. After the deposition of the thin films, biaxial compressive residual stresses in the thin film plane were observed in our samples. Over the last several decades, numerous theoretical and experimental studies of this phenomenon have been performed 1 17. Buckling and postbuckling of a compressed thin film bonded on a.
Compressed thin films deposited on substrates may buckle depending on the geometrical and mechanical properties of the film substrate set. The mechanically guided assembly that relies on the compressive buckling of strategically patterned 2d thin films represents a robust route to complex 3d m based on this approach, formation of complex 3d configurations with suspended curvy features or hierarchical geometries remains a challenge. Threedimensional silicon electronic systems fabricated by. The critical compressive strain and buckling wavelength for the sinusoidal mode are obtained analytically for the case with the substrate modulus decaying exponentially. E x axial stiffness in the direction of compressive loading g xz shear stiffness in the throughthethickness direction direction of buckling. For structures consisting of a thin film bonded to a compliant substrate, wrinkling of the thin film is commonly observed as a result of mechanical instability. The changeover from yielding to buckling failure occurs at the point c, defined by a slenderness ratio given by. Direct numerical simulation of buckling instability of. Two buckling modes have been observed in thin films. In these systems, controlled buckling is realized in thin films deposited, typically by vapor phase or physical transfer processes, onto prestrained elastomeric substrates. Under none to minor compression, the film does not buckle and remains flat fig. Motivated by the deficiencies of the current 2d models, the goal of this paper is to demonstrate a computational multiscale 3d finite element simulation of the. In the case of compressive stress thin film buckling is observed in the form of delamination blisters, which can be either circular, straight, or form periodic buckling patterns commonly known as telephone cord delamination morphology.
Suspended square membranes undergo at least two buckling transitions. Herringbone buckling patterns of compressed thin films on. Methods and fabrication processes of realizing stretchability in different thin films, such as semiconductors, metals, and polymers, on compliant substrates are introduced. Ridge localizations and networks in thin films compressed. Wrinkleamplitude equilibrium amplitude increases with. As a result the compressive force and the total longitudinal strain of sublaminate are expressed in terms of complete elliptic integrals, which uniquely identify the buckled shape of sublaminate, the effect of buckling on the compression strain and increment of the compressive force in the buckled state. Em397 thin films term paper fall 2006 haixia mei effects of substrate compliance on buckling delamination of thin films under compression abstract. The general phenomena shown in delamination buckles of compressively stressed films were discussed from the onset to propagation over the substrates. The strain energy release rate at the cracktip g is derived in terms of the critical equivalent base laminate strain at the onset of the buckling. Attractive features include applicability to wide ranging layout designs and dimensions along with the capacity to integrate planar thin film materials and device layouts. Stress and moisture effects on thin film buckling delamination. When the compressive stress in the film w, the film buckles spontaneously.
As a result the compressive force and the total longitudinal strain of sublaminate are expressed in terms. Assembly of micronanomaterials into complex, three. Direct numerical simulation of buckling instability of thin. Although many theoretical models exist for postbuckling behavior in thinfilm structures, 19,4649 they focus mainly on the single process of compressive buckling and cannot be used directly. Buckling delamination of compressed thin films springerlink. We take a variational viewpointfocusing on the total elastic energy, i. Buckling and cracking of thin films on compliant substrates under. Detailed modelling of delamination buckling of thin films. Compressive stresses may initiate film buckling while highly tensile stresses can result in film cracking. The mechanically guided assembly that relies on the compressive buckling of strategically patterned 2d thin films represents a robust route to complex 3d mesostructures in advanced materials and even functional microdevices. The mechanisms whereby these debonding patterns interact have been investigated taking into account the elastic. Unstable with any compressive stress in a thin film lh 1. Buckling, wrinkling and debonding in thin film systems abstract. Buckling, wrinkling and debonding in thin film systems ieee.
Experiments have shown that buckling and the associated delamination process are initiated and driven by interfacial shear in addition to compressive stresses in the film. Herringbone buckling patterns of compressed thin films on compliant substrates. The film demonstrates good mechanical flexibility facilitating reliable transfer. Buckling of a stiff thin film on a compliant substrate in.
In the region ac, where the slenderness values are low, the column fails by yielding. Thin film buckling buckle generally considered refers to a failure mode caused by the compressive force on the film material, characterized by the vertical displacement perpendicular to load direction. Ridge localizations and networks in thin films compressed by. Instead, the film supports a small compressive strain pre, which we refer to as membrane strain. Residual compressive stresses are often induced in thin films because of the mismatch. Mar 31, 2020 for structures consisting of a thin film bonded to a compliant substrate, wrinkling of the thin film is commonly observed as a result of mechanical instability. The films were analyzed in situ by a cantilever beam technique, and ex situ by atomic force microscopy afm and focused ion beam. In these systems, many times, the mismatch in the coefficient of thermal expansion between the films and the substrate result in significant compressive stresses during processing. Recently developed approaches in deterministic assembly allow for controlled, geometric transformation of twodimensional structures into complex, engineered threedimensional layouts. Thin walled, coldformed steel members exhibit a complicated post buckling regime that is difficult to predict. Finite deformation mechanics in buckled thin films.
Combination of weak adhesion and compressive stresses results in buckling driven delamination of the film, leaving blisters on the glass surface. Effects of substrate compliance on buckling of thin films under. Buckling modes of elastic thin films on elastic substrates. Stress relaxation related to spontaneous thin film.
Thin film modeling of delamination buckling in pressure loaded laminated cylindrical shells. Large compressive stress in combination with insufficient adhesion at the interface often leads to local or global film buckling and delamination. We first introduce the mechanism of developing wave patterns through buckling using beam. The mechanical and interfacial properties of metal films on polymer substrates under combined loading directly affect the function and service life of a variety of devices. Buckling of thin films in nanoscale semantic scholar. The wavy patterns are generated when the thin elastic film is subjected to an inplane compressive stress and by the application of controlled heating. Depending on the magnitude of compressive strain in thin films, different types of buckling patterns were observed. Spontaneous formation of ordered structures in thin films. In situ atomic force microscopy observations have been carried out of thin films under external compressive stress. Spontaneous formation of ordered structures in thin films of. Compressed thin films deposited on substrates may buckle depending on the geometrical and mechanical properties of the filmsubstrate set. Anticipated buckling or compressive failure forces will first be calculated for various length specimens and materials. In this exercise, two materials and two column lengths will be studied.
Mesoscale xray diffraction measurement of stress relaxation. Reprogrammable 3d mesostructures through compressive buckling. Stress relaxation related to spontaneous thin film buckling. Spontaneous delamination via compressive buckling facilitates large. Novel applications that are enabled by stretchable thin films are presented. As the temperature drops and the compressive stresses in the film increase, buckling starts where the maximum principal compressive stress attains the critical value. Thin film buckling, wrinkling, ridge localization, substrate prestretch, ridge networks the intriguing buckling patterns exhibited by bilayer systems composed of a thin stiff film bonded to a thick elastomeric substrate have been studied extensively in recent years both experimentally and theoretically. Membrane and peak strains in the film due to the prestrain. Buckling of composite material compression specimens. This is demonstrated experimentally by observing both the buckling modes and a mode transition in a single film substrate system with varying stress and interfacial defects. In the region cb, the failure will be triggered by buckling. Pdf postbuckling shear strength of thin steel plates.
Mechanicalthermal response of brittle titanium films on. An understanding of such a twolevel buckling phenomenon is essential for optimal design of processing parameters related to this approach. Effects of substrate compliance on buckling of thin films. A thin metal film vapor deposited on thick elastomer substrate develops an equibiaxial compressive stress state when the system is cooled due to the large thermal expansion mismatch between the elastomer and the metal. Analysis of a compressed thin film bonded to a compliant. The residual stresses were far beyond the critical stresses, under which the films will be debonded and buckled away from the substrates. Compressive buckling of laminates with an embedded delamination. Nov 09, 2004 at a critical stress, the film undergoes buckling into a family of modes with short wavelengths characteristic of a thin plate on a compliant elastic foundation. Nonlinear buckling of thin, high modulus plates on compliant supports represents a classic problem in mechanics. May 06, 2010 buckling, wrinkling and debonding in thin film systems abstract. Thin films bonded to substrates commonly occur in semiconductor dielectric stacks. Wrinkleamplitude equilibrium amplitude increases with the stressstrain.
260 798 1251 742 51 527 957 845 1058 1061 426 928 137 322 1174 1354 874 494 911 1492 727 183 763 833 1236 680 1380 778 916 1005 448 644 374 190 402 461 491 585 10 549 768 1215 88 1021 1283 268